Targeted Depositions

NREL has several non-combinatorial physical vapor deposition chambers for targeted follow-up studies of the most promising materials identified by combinatorial synthesis.

Molecular Beam Epitaxy

Molecular beam chamber: No. 1

Materials: Oxides, Nitrides

Substrates: <4" diameter, <1200C

Sources: 8 effusion cells

Gases: O and N RF plasma

Base pressure: 10-11-10-10 Torr

Features: Load lock, preparation chamber, reflection high-energy electron diffraction, oxygen-resistant substrate heater, and laser reflectometry

Publications:

Growth and Characterization of Homoepitaxial ß-Ga2O3 Layers, J. Phys. D: Appl. Phys. 5 (2020)

Heteroepitaxial Integration of ZnGeN2 on GaN Buffers Using Molecular Beam Epitaxy
Cryst. Growth Des. (2020)

Photo of molecular beam chamber

Pulsed Laser Deposition

Pulsed laser deposition chamber: No. 1

Materials: Oxides and other materials

Substrates: <3" diameter, <800C

Targets: 1” circular

Gases: Ar, O, N, N2/H2

Base pressure: 10-9-10-8 Torr

Features: Targeted material deposition

Publications:

Li-Doped Cr2MnO4: A New p-Type Transparent Conducting Oxide by Computational Materials Design, Adv. Funct. Mat. (2013)

Control of the Electrical Properties in Spinel Oxides by Manipulating the Cation Disorder, Adv. Func. Mat. (2014)

Photo of pulsed laser deposition chamber

Pulsed laser deposition chamber: No. 2

Materials: Oxides

Substrates: <3" diameter, <800C

Targets: 1” circular

Gases: Ar, O, N, N2/H2

Base pressure: 10-9-10-8 Torr

Features: Targeted material deposition and load lock

Publications:

Enhanced Electron Mobility Due to Dopant-Defect Pairing in Conductive ZnMgO, Adv. Func. Mat. (2014)

Surface Origin of High Conductivities in Undoped In2O3 Thin Films, Phys. Rev. Lett. (2012)

 Photo of pulsed laser deposition chamber

Additional Publications

Growth and Characterization of Homoepitaxial ß-Ga2O3 Layers, J. Phys. D: Appl. Phys. (2020)

Epitaxial Growth of Rock Salt MgZrN2 Semiconductors on MgO and GaN, Applied Physics Letters (2020)

Heteroepitaxial Integration of ZnGeN2 on GaN Buffers Using Molecular Beam Epitaxy, Crystal Growth and Design (2020)

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